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51

Chemistry of iridium carbonyl cluster complexes. Synthesis and x-ray crystal structure of bis(tetraphenylphosphonium) octa-.mu.-carbonyloctadecacarbonyldodecairidate(2-), the first example of a medium-size iridium carbonyl cluster complex

Della Pergola, Roberto, Demartin, Francesco, Garlaschelli, Luigi, Manassero, Mario, Martinengo, Secondo, Sansoni, Mirella

Journal:

Inorganic Chemistry

Year:

1987

Language:

english

File:

PDF, 671 KB

english, 1987

52

Chemistry of iridium carbonyl cluster complexes. Synthesis and x-ray crystal structure determination of the [NMe3(CH2Ph)]3[Ir9(.mu.-CO)7(CO)13] complex containing a cofacial bioctahedral iridium cluster. Another example of different electron counting between isoskeletal rhodium and iridium carbonyl clusters

Della Pergola, Roberto., Demartin, Francesco., Garlaschelli, Luigi., Manassero, Mario., Martinengo, Secondo., Masciocchi, Norberto., Strumolo, Donatella.

Journal:

Inorganic Chemistry

Year:

1991

Language:

english

File:

PDF, 552 KB

english, 1991

53

Reactivity of Rh4(CO)12 with halides or pseudohalides: synthesis of the pentanuclear carbonyl clusters [Rh5(CO)14X]n- (X = Cl, Br, I, SCN, n = 2; X = PPh3, n = 1). Crystal structures of [N(PPh3)2][Rh5(.mu.-CO)6(CO)8(PPh3)] and [N(PPh3)2]2[Rh5(.mu.-CO)6(CO)8(SCN)]

Fumagalli, Alessandro, Martinengo, Secondo, Galli, Daniele, Allevi, Claudio, Ciani, Gianfranco, Sironi, Angelo

Journal:

Inorganic Chemistry

Year:

1990

Language:

english

File:

PDF, 768 KB

english, 1990

54

Chemistry of iridium carbonyl cluster complexes. Synthesis and x-ray crystal structure of [PPh4]2[Ir12(.mu.-CO)5(CO)19], containing an unprecedented metal skeleton

Della Pergola, Roberto, Demartin, Francesco, Garlaschelli, Luigi, Manassero, Mario, Martinengo, Secondo, Masciocchi, Norberto, Zanello, Piero

Journal:

Inorganic Chemistry

Year:

1993

Language:

english

File:

PDF, 635 KB

english, 1993

55

Carbon-13 nuclear magnetic resonance of pentadecacarbonylcarbylhexarhodate(2-)

Albano, Vincenzo G., Chini, Paolo, Martinengo, Secondo, McCaffrey, David J. A., Strumolo, Donatella, Heaton, Brian T.

Journal:

Journal of the American Chemical Society

Year:

1974

Language:

english

File:

PDF, 213 KB

english, 1974

56

Characterization of the Solid−Solid Phase Transition of Co 2 (CO) 6 (AsPh 3 ) 2

Macchi, Piero, Garlaschelli, Luigi, Martinengo, Secondo, Sironi, Angelo

Journal:

Inorganic Chemistry

Year:

1998

Language:

english

File:

PDF, 99 KB

english, 1998

57

Synthesis and x-ray structural characterization of the [Rh22(.mu.3-CO)7(.mu.-CO)18(CO)12]4- anion, containing a large close-packed cluster with an ABAC sequence of compact layers

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the American Chemical Society

Year:

1980

Language:

english

File:

PDF, 240 KB

english, 1980

58

Skeletal Growth by Condensation of Small Metal Fragments on a Carbido Carbonyl Cluster. Synthesis of the Anions [Rh 15 C 2 (CO) 24 X 2 ] 3- (X = Cl, Br, I) and Molecular Structure of the Bromo and Iodo Derivatives

Fumagalli, Alessandro, Martinengo, Secondo, Bernasconi, Giovanni, Noziglia, Luciana, Albano, Vincenzo G., Monari, Magda, Castellari, Carlo

Journal:

Organometallics

Year:

2000

Language:

english

File:

PDF, 86 KB

english, 2000

59

Stabilization of carbonyl clusters by a carbide atom. Synthesis and characterization of carbonoctadecacarbonyloctacobaltate(2-) and of paramagnetic carbontetradecacarbonylhexacobaltate(1-) anions

Albano, Vincenzo G., Chini, Paolo, Ciani, Gianfranco, Sansoni, Mirella, Strumolo, Donatella, Heaton, Brian T., Martinengo, Secondo

Journal:

Journal of the American Chemical Society

Year:

1976

Language:

english

File:

PDF, 267 KB

english, 1976

60

Tri(.pi.-allyl)iridium(III)

Chini, Paolo, Martinengo, Secondo

Journal:

Inorganic Chemistry

Year:

1967

Language:

english

File:

PDF, 287 KB

english, 1967

61

A mixed-metal nitridocarbonyl cluster compound. Synthesis and x-ray structure of the [PtRh10N(.mu.-CO)10(CO)11]3- anion

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the American Chemical Society

Year:

1982

Language:

english

File:

PDF, 373 KB

english, 1982

62

New carbide clusters in the cobalt sub-group. Part 14. Synthesis and structural characterization of the anion [Co13C2(CO)24]3? as its benzyltrimethylammonium salt

Albano, Vincenzo G., Braga, Dario, Fumagalli, Alessandro, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1985

Language:

english

File:

PDF, 468 KB

english, 1985

63

New arrangements of transition metal atoms in carbido-carbonyl clusters of rhodium and cobalt

Albano, Vincenzo G., Chini, Paolo, Martinengo, Secondo, Sansoni, Mirella, Strumolo, Donatella

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1974

Language:

english

File:

PDF, 225 KB

english, 1974

64

A novel high-nuclearity rhodium carbonyl cluster compound containing two interstitial nitrogen atoms: synthesis and X-ray structure of the anion [Rh14N2(CO)25]2?

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1991

Language:

english

File:

PDF, 384 KB

english, 1991

65

New carbide clusters in the cobalt sub-group. Part III. Crystallographic characterization of the hydroxonium salt of tetradeca-�-carbonyl-dicarbidotetradecacarbonyl-polyhedro-pentadecarhodate(1?)

Albano, Vincenzo G., Sansoni, Mirella, Chini, Paolo, Martinengo, Secondo, Strumolo, Donatella

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1976

Language:

english

File:

PDF, 680 KB

english, 1976

66

Synthesis and X-ray characterization of the novel [Rh10S(CO)10(�-CO)12]2? anion; a bicapped square-antiprismatic cluster containing an interstitial sulphur atom

Ciani, Gianfranco, Garlaschelli, Luigi, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1981

Language:

english

File:

PDF, 283 KB

english, 1981

67

High nuclearity carbonyl clusters of rhodium. Part 2. Crystal and molecular structure of the tetramethylammonium salt of dodeca-�-carbonyl-dodecacarbonylhydrido-polyhedro-tridecarhodate(4?)?1-methylpyrrolidin-2-one (1/3)

Ciani, Gianfranco, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1981

Language:

english

File:

PDF, 611 KB

english, 1981

68

High nuclearity Pt?Rh carbonyl clusters. Synthesis and X-ray characterization of the [Pt2Rh11(�-CO)12(CO)12]3? and [PtRh12(�-CO)12(CO)12]4? anions

Fumagalli, Alessandro, Martinengo, Secondo, Ciani, Gianfranco

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1983

Language:

english

File:

PDF, 283 KB

english, 1983

69

13C nuclear magnetic resonance of triacontacarbonyldodecarhodate(2?): [Rh12(CO)20(�2-CO)2-(�3-CO)8]2?

Chini, Paolo, Martinengo, Secondo, McCaffrey, David J. A., Heaton, Brian T.

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1974

Language:

english

File:

PDF, 160 KB

english, 1974

70

A large rhodium carbonyl cluster compound containing four encapsulated nitrogen atoms: synthesis and X-ray structure of the anion [Rh23N4(CO)20(�-CO)18]3?

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1992

Language:

english

File:

PDF, 324 KB

english, 1992

71

Mixed-metal carbido carbonyl clusters. Part 4. Synthesis and structural characterization of [Rh6C(CO)13{Au2(PPh3)2}]

Fumagalli, Alessandro, Martinengo, Secondo, Albano, Vincenzo G., Braga, Dario, Grepioni, Fabrizia

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1989

Language:

english

File:

PDF, 600 KB

english, 1989

72

Synthesis and X-ray crystal structure of the novel cluster anion [Rh12H(N)2(CO)23]3?; an irregular metallic array containing two interstitial nitrogen atoms

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1986

Language:

english

File:

PDF, 303 KB

english, 1986

73

Synthesis and X-ray characterization of the high-nuclearity [Rh17(�3-CO)3-(�-CO)15(CO)12]3? anion containing a tetracapped twinned cuboctahedral cluster

Ciani, Gianfranco, Magni, Ambrogio, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1981

Language:

english

File:

PDF, 265 KB

english, 1981

74

New carbide clusters in the cobalt subgroup. Part 12. Synthesis and X-ray characterization of the tetradecanuclear carbido-carbonyl cluster [Rh14C2(�-CO)21(CO)12]2?

Martinengo, Secondo, Strumolo, Donatella, Chini, Paolo, Albano, Vincenzo G., Braga, Dario

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1984

Language:

english

File:

PDF, 650 KB

english, 1984

75

Mixed-metal carbido carbonyl clusters. Part 1. Synthesis and structural characterization of Di-�3-acetonitrilecuprio-carbido-ennea-�-carbonyl-hexacarbonyl-polyhedro-hexarhodium, [Cu2Rh6(CO)15(NCMe)2]�0.5MeOH

Albano, Vincenzo G., Braga, Dario, Martinengo, Secondo, Chini, Paolo, Sansoni, Mirella, Strumolo, Donatella

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1980

Language:

english

File:

PDF, 443 KB

english, 1980

76

Synthesis and X-ray crystal structure of the cluster dianion, [Rh10(CO)21]2?, containing a new compact array of metal atoms

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1986

Language:

english

File:

PDF, 259 KB

english, 1986

77

New carbide clusters in the cobalt sub-group. Part 10. Preparation and crystallographic characterization of dicarbido-octa-�-carbonyl-hexadecacarbonyl-polyhedro-dodecarhodate(2?) as its bis(triphenyl-phosphine)iminium salt, [N(PPh3)2]2[Rh12C2(CO)24]

Albano, Vincenzo G., Braga, Dario, Chini, Paolo, Strumolo, Donatella, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1983

Language:

english

File:

PDF, 531 KB

english, 1983

78

Rhodium carbonyl clusters with interstitial nitrogen atoms. Part 1. Crystal and molecular structure of the bis(triphenylphosphine)iminium salt of the anion ennea-�-carbonyl-hexacarbonyl-�6-nitrido-polyhedro-hexarhodate(1?)

Bonfichi, Riccardo, Ciani, Gianfranco, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1983

Language:

english

File:

PDF, 487 KB

english, 1983

79

Vibrational frequencies associated with the interstitial atom in [M6(CO)15C]2? and [M6(CO)15N]?(M = Co or Rh)

Creighton, J. Alan, Pergola, Roberto Della, Heaton, Brian T., Martinengo, Secondo, Strona, Luisella, Willis, David A.

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1982

Language:

english

File:

PDF, 217 KB

english, 1982

80

Synthesis and X-ray crystal structure of the cluster compound [Rh12H2(�3-CO)3(�-CO)9(CO)13] containing a metallic array formed by three superimposed cofacial octahedral units

Ciani, Gianfranco, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1985

Language:

english

File:

PDF, 304 KB

english, 1985

81

A case of solid?state isomerism for a rhodium carbonyl cluster anion. Synthesis, characterization in solution and X-ray crystallographic structures of the salts [NMe4]3[Rh11(CO)23]�Me2CO and [NMe4]3[Rh11(CO)23]�C6H5Me

Fumagalli, Alessandro, Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo, Heaton, Brian T.

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1988

Language:

english

File:

PDF, 1.11 MB

english, 1988

82

Reactions of the nitridocarbonyl cluster anion [Rh6N(CO)15]? with strong bases: synthesis and crystal structure of the hydridic dianion [Rh6(�-H)N(CO)14]2?

Ciani, Gianfranco, Proserpio, Davide M., Sironi, Angelo, Martinengo, Secondo, Fumagalli, Alessandro

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1994

Language:

english

File:

PDF, 699 KB

english, 1994

83

Synthesis and X-ray crystal structure of the novel high nuclearity rhodium-cluster dianion [Rh14(�-CO)15(CO)11]2?

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1980

Language:

english

File:

PDF, 318 KB

english, 1980

84

The synthesis and nuclear magnetic resonance spectroscopic study of [Rh10S(CO)22]2?

Garlaschelli, Luigi, Fumagalli, Alessandro, Martinengo, Secondo, Heaton, Brian T., O. Smith, David, Strona, Luisella

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1982

Language:

english

File:

PDF, 353 KB

english, 1982

85

Synthesis and chemical characterization of the new anions [Rh3(�3-E)2(CO)6]?(E = S or Se). Crystal and molecular structures of [PPh4][Rh3(�3-S)2(CO)6] and [NMe4][Rh3(�3-Se)2(CO)6]

Galli, Daniele, Garlaschelli, Luigi, Ciani, Gianfranco, Fumagalli, Alessandro, Martinengo, Secondo, Sironi, Angelo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1984

Language:

english

File:

PDF, 1.04 MB

english, 1984

86

Use of supported rhodium and cobalt carbonyls as catalysts for the CO + H2 reaction. Effect of the support and the metal

Ceriotti, Alessandro, Martinengo, Secondo, Zanderighi, Luciano, Tonelli, Claudio, Iannibello, Antonio, Girelli, Alberto

Journal:

Journal of the Chemical Society Faraday Transactions 1

Year:

1984

Language:

english

File:

PDF, 760 KB

english, 1984

87

Chemistry of iridium carbonyl clusters. Synthesis and chemical characterization of the hexanuclear anions [Ir6(CO)15(CO2R)]?(R = Me or Et) and [Ir6(CO)14(CO2Me)2]2?. Crystal and molecular structure of [N(PPh3)2][Ir6(�-CO)4(CO)11(CO2Me)]

Garlaschelli, Luigi, Malatesta, Maria Carlotta, Martinengo, Secondo, Demartin, Francesco, Manassero, Mario, Sansoni, Mirella

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1986

Language:

english

File:

PDF, 783 KB

english, 1986

88

Synthesis and chemical characterization of the chalcogenide capped iridium carbonyl anions: [Ir3(�3-X)2(CO)6]?(X = S or Se). Crystal and molecular structures of [NMe3(CH2Ph)][Ir3(�3-S)2(CO)6] and [NMe4][Ir3(�3-Se)2(CO)6]

Pergola, Roberto Della, Garlaschelli, Luigi, Martinengo, Secondo, Demartin, Francesco, Manassero, Mario, Sansoni, Mirella

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1986

Language:

english

File:

PDF, 707 KB

english, 1986

89

Isoskeletal Rh10C2 metal clusters containing four Au(PPh3) groups and a variable number of carbonyl ligands

Fumagalli, Alessandro, Martinengo, Secondo, Albano, Vincenzo G., Braga, Dario, Grepioni, Fabrizia

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1993

Language:

english

File:

PDF, 746 KB

english, 1993

90

High nuclearity carbonyl clusters of rhodium. Part 1. Crystallographic characterization of dodeca-�-carbonyl-dodecacarbonyldihydrido-polyhedro-tridecarhodate(3?) in its benzyltriphenylphosphonium salt

Albano, Vincenzo G., Ciani, Gianfranco, Martinengo, Secondo, Sironi, Angelo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1979

Language:

english

File:

PDF, 573 KB

english, 1979

91

Synthesis and chemical characterization of the hexanuclear anions [Ir6(CO)14X]?(X = Cl, Br, I, or SCN). Crystal and molecular structures of [PPh4][Ir6(�-CO)2(CO)12(�-Br)] and [N(PPh3)2][Ir6(�-CO)12(�-X)](X = I or SCN)

Pergola, Roberto Della, Garlaschelli, Luigi, Martinengo, Secondo, Demartin, Francesco, Manassero, Mario, Masciocchi, Norberto

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1988

Language:

english

File:

PDF, 963 KB

english, 1988

92

High nuclearity carbonyl clusters of rhodium. Part 3. Crystal and molecular structure of hexadeca-�-carbonyl-enneacarbonyl-polyhedro-tetradecarhodate(4?) in its tetraethylammonium salt

Ciani, Gianfranco, Sironi, Angelo, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1982

Language:

english

File:

PDF, 486 KB

english, 1982

93

An octanuclear iridum carbonyl cluster based on two equivalent tetrahedral units. Synthesis and X-ray characterization of bis(tetraphenylphosphonium) hexa-�-carbonylhexadecacarbonyl-ditetrahedro-octairidate (2?)

Demartin, Francesco, Manassero, Mario, Sansoni, Mirella, Garlaschelli, Luigi, Raimondi C., Carlo, Martinengo, Secondo, Canziani, Franco

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1981

Language:

english

File:

PDF, 247 KB

english, 1981

94

New carbide clusters in the cobalt sub-group. Part 6. Crystallographic characterization of the tetramethylammonium salt of the paramagnetic anion carbidohexa-�-carbonyl-octacarbonyl-polyhedro-hexa-cobaltate(1?)

Albano, Vincenzo G., Chini, Paolo, Ciani, Gianfranco, Sansoni, Mirella, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1980

Language:

english

File:

PDF, 435 KB

english, 1980

95

Mixed-metal carbido carbonyl clusters. Part 3. Synthesis and structural characterization of [Rh6C(CO)15{Ag(NCMe)}2]�0.5MeOH, [Rh6C(CO)15{M-(PPh3)}2](M = Cu, Ag, or Au), and of the anion [Rh6C(CO)15{Au(PPh3)}]? as its PPh4 + salt

Fumagalli, Alessandro, Martinengo, Secondo, Albano, Vincenzo G., Braga, Dario

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1988

Language:

english

File:

PDF, 1.40 MB

english, 1988

96

A new family of nitrido carbonyl clusters. Synthesis and structural characterization of the anions [Rh6MN(CO)15]2?(M?Co, Rh, or Ir), and evidence for metal atom migration in the cluster

Martinengo, Secondo, Ciani, Gianfranco, Sironi, Angelo

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1984

Language:

english

File:

PDF, 281 KB

english, 1984

97

Hexanuclear rhodium hydrido-carbonyl clusters

Heaton, Brian T., Strona, Luisella, Martinengo, Secondo, Strumolo, Donatella, Goodfellow, Robin J., Sadler, Ian H.

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1982

Language:

english

File:

PDF, 470 KB

english, 1982

98

New carbide clusters in the cobalt sub-group. Part 15. Synthesis and crystallographic characterization of di-�6-carbido-deca-�-carbonyl-tridecacarbonyl-polyhedro-dodecarhodate(4?) as its tetrapropylammonium salt, [N(C3H7)4]4[Rh12C2(CO)23]

Albano, Vincenzo G., Braga, Dario, Strumolo, Donatella, Seregni, Claudio, Martinengo, Secondo

Journal:

Journal of the Chemical Society Dalton Transactions

Year:

1985

Language:

english

File:

PDF, 670 KB

english, 1985

99

A new synthesis and the X-ray crystal structure of bis(trimethylbenzylammonium) tri-�-carbonyl-dodecacarbonyl-octahedro-hexairidate(2?)

Demartin, Francesco, Manassero, Mario, Sansoni, Mirella, Garlaschelli, Luigi, Martinengo, Secondo, Canziani, Franco

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1980

Language:

english

File:

PDF, 281 KB

english, 1980

100

Bismuth?cobalt heteronuclear carbonyl cluster compounds. Synthesis and X-ray characterization of the neutral [BiCo3(CO)9] and of the paramagnetic anion [Bi2Co4(CO)11]?

Martinengo, Secondo, Ciani, Gianfranco

Journal:

Journal of the Chemical Society Chemical Communications

Year:

1987

Language:

english

File:

PDF, 355 KB

english, 1987

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