Metal-promoted alkyne trimerisation leading to novel metallacycles. The molecular structures of [Mo{?3-C(CF3)C(CF3)C(Me)?C(Ph)SPri}(CF3C?CCF3)(?5-C5H5)], [WSPri{?5-C(CF3)C(CF3)C(CF3)?C(CF3)C(Me)?C(Ph)}(?5-C5H5)], and [W(SC6H4Me-4){?4-C(CF3)?C(CF3)C(CO2Me)?C(CO2Me)C(CF3)?C(CF3)}(?5-C5H5)]

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