The mild phase transfer syntheses of the ylide adduct (CO)4F−eCH2P+Ph3, the octacarbonyl(μ-methylene)diiron μ-CH2Fe2(CO)8, and acyl tetracarbonyliron anions RCOFe(CO)4− are consistent with the transient generation of the Fe(CO)42− dianion from Fe(CO)5

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