An Approach to the Precise Chemoenzymatic Synthesis of 13 C-Labeled Sialyloligosaccharide on an Intact Glycoprotein:  A Novel One-Pot [3- 13 C]-Labeling Method for Sialic Acid Analogues by Control of the Reversible Aldolase Reaction, Enzymatic Synthesis of [3- 13 C]-NeuAc-α-(2→3)-[U- 13 C]-Gal-β-(1→4)-GlcNAc-β- Sequence onto Glycoprotein, and Its Conformational Analysis by Developed NMR Techniques