Stabilization of high-valent transition-metal complexes with macrocyclic tertiary amines. Reinvestigation of the synthesis, electrochemistry, and spectroscopy of osmium(III) macrocyclic amine complexes and x-ray crystal structure of trans-[OsIII(16-TMC)Cl2]ClO4 (16-TMC = 1,5,9,13-tetramethyl-1,5,9,13-tetraazacyclohexadecane)

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