Tirucalla-5,24-dien-3?-ol [(13?,14?,17?,20S)-lanosta-5,24-dien-3?-ol] and three other ?5-unsaturated tirucallanes from the roots of Bryonia dioica Jacq.: the first naturally occurring C-10 methylated tetracyclic triterpene alcohols with a ?5-monounsaturated skeleton

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