Macrocyclic nickel(II) complexes with a folded conformation. Synthesis, properties and structures of [NiL(en)][Ni(en)3](ClO4)4 and [(NiL)2(μ-ox)](ClO4)2 (L=3,10-bis(2-hydroxyethyl)-1,3,5,8,10,12-hexaazacyclotetradecane, en=ethylenediamine, ox=oxalate anion)

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