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Facile Reduction of Early Transition Metal Halides with Nonconventional, Mild Reductants. Part 5. Gallium and Gallium Dichloride, New Solid-State Reductants in Preparative Transition Metal Chemistry. New, Lower Temperature Syntheses and Convenient Isolation of Hexatantalum Tetradecachloride Octahydrate, Ta6(μ-Cl)12Cl2 (OH2)4×4H2O, and Synthesis and Solid-State Structure of a Tetraalkylammonium Derivative, [N(CH2Ph)Bu3]4 [Ta6(μ-Cl)12Cl6], of the Reduced [Ta6(μ-Cl)12]2+ Cluster Core.
Daniel N. T. Hay, Dale C. Swenson, Louis MesserleVolume:
33
Year:
2002
Language:
english
Pages:
1
DOI:
10.1002/chin.200246020
File:
PDF, 40 KB
english, 2002