Volume 12; Issue 1

Organic Process Research & Development

Volume 12; Issue 1

1

Some Items of Interest to Process R&D Chemists and Engineers

Rubio, Silvina García, Pfeiffer, Matthew, Tilstam, Ulf, Antunes, Octavio Augusto Ceva, Laird, Trevor, Zlota, Andrei A., McLaughlin, Mark

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 270 KB

english, 2008

2

First Scale-Up: Problems and Resolutions on the Synthesis of WAY-253752, a Novel, Dual-Acting SSRI/5HT1A Antagonist

Nikitenko, Antonia, Evrard, Deborah, Sabb, Annmarie L., Vogel, Robert L., Stack, Gary, Young, Mairead, Lin, Melissa, Harrison, Boyd L., Potoski, John R.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 142 KB

english, 2008

3

Large-Scale Preparation of 2-Methyloxazole-4-carboxaldehyde

Benoit, Georges-Emmanuel, Carey, John S., Chapman, Alan M., Chima, Ranjit, Hussain, Nigel, Popkin, Matthew E., Roux, Guillaume, Tavassoli, Bahareh, Vaxelaire, Carine, Webb, Michael R.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 139 KB

english, 2008

4

An Investigation on Key Parameters That Influence the Resolution of Omeprazole Sodium †

Reddy, Lekkala Amarnath, Malakondaiah, Golla China, Babu, Karrothu Srihari, Bhattacharya, Apurba, Bandichhor, Rakeshwar, Himabindu, Vimmidi, Reddy, Padi Pratap, Anand, Ramasamy Vijaya

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 118 KB

english, 2008

5

Development of a Practical Route for the Manufacture of N -[5-(3-Imidazol-1-yl-4-methanesulfonyl-phenyl)-4-methyl-thiazol-2-yl]acetamide

Hirt, Hans, Haenggi, Ruedi, Reyes, Jesus, Seeger-Weibel, Manuela, Gallou, Fabrice

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 127 KB

english, 2008

6

An Efficient and Practical Synthesis of the HIV Protease Inhibitor Atazanavir via a Highly Diastereoselective Reduction Approach

Fan, Xing, Song, Yan-Li, Long, Ya-Qiu

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 205 KB

english, 2008

7

Sulfur Contamination Due to Quenching of Halogenation Reactions with Sodium Thiosulfate: Resolution of Process Problems via Improved Quench Protocols

Xiang, Yanqiao, Caron, Pierre-Yves, Lillie, Brett M., Vaidyanathan, Rajappa

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 118 KB

english, 2008

8

Process Development of TRI-999, a Fatty-Acid-Modified HIV Fusion Inhibitory Peptide

Zhang, Huyi, Schneider, Stephen E., Bray, Brian L., Friedrich, Paul E., Tvermoes, Nicolai A., Mader, Catherine J., Whight, Sheila R., Niemi, Toivo E., Silinski, Peter, Picking, Tony, Warren, Marquitta

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 1.71 MB

english, 2008

9

Approaches for Scale-Up of Microwave-Promoted Reactions

Bowman, Matthew D., Holcomb, Jennifer L., Kormos, Chad M., Leadbeater, Nicholas E., Williams, Victoria A.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 1.81 MB

english, 2008

10

A Comparison of Commercial Microwave Reactors for Scale-Up within Process Chemistry

Moseley, Jonathan D., Lenden, Philip, Lockwood, Mark, Ruda, Katinka, Sherlock, Jon-Paul, Thomson, Anthony D., Gilday, John P.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 205 KB

english, 2008

11

Process Research on the Preparation of 1-(3-Trimethylsilylphenyl)-2,2,2-trifluoroethanone by a Friedel–Crafts acylation Reaction

Wolf, Richard A.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 136 KB

english, 2008

12

Chris Schmid Resigns as Associate Editor; Jaan Pesti (BMS) Is Appointed as New Associate Editor from 1 December 2007

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 48 KB

english, 2008

13

Implementation on Pilot-Plant Scale of the Titanocene-Catalyzed Reduction of a Lactone with Poly(methylhydrosiloxane)

Depré, Dominique, Horváth, András, Snissaert, Walter, Bergh, Leo Van Den, Dermaut, Wim

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 679 KB

english, 2008

14

Adsorbent Screening Using Microplate Spectroscopy for Selective Removal of Colored Impurities from Active Pharmaceutical Intermediates

Welch, Christopher J., Leonard, William R., Henderson, Derek W., Dorner, Benjamin, Childers, Karla Glaser, Chung, John Y. L., Hartner, Frederick W., Albaneze-Walker, Jennifer, Sajonz, Peter

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 1.70 MB

english, 2008

15

Purification of 2,4 Dichlorobenzoic Acid

Ley, Christopher P., Yates, Matthew H.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 970 KB

english, 2008

16

New Synthetic Approach to Memantine Hydrochloride Starting from 1,3-Dimethyl-adamantane

Madhra, Mukesh K., Sharma, Mukesh, Khanduri, C. H.

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 34 KB

english, 2008

17

Synthesis of Tetracyclic Heterocompounds as Selective Estrogen Receptor Modulators. Part 2. Process Improvement for Scale-Up of 2,5,8-Substituted 11,12-Dihydro-5 H -6,13-dioxabenzo[3,4]cyclohepta-[1,2- a ]naphthalene Derivatives

Li, Xun, Reuman, Michael, Russell, Ronald K., Youells, Scott, Beish, Sandra, Hu, Zhiyong, Branum, Shawn, Jain, Nareshkumar, Sui, Zhihua

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 34 KB

english, 2008

18

Organic Syntheses, Volume 84. Marvin J. Miller , Ed. Organic Syntheses Inc./Wiley : New York . 2007 . 371 + li pages. £31.95. ISBN 978-0-470-09901-8 .

Journal:

Organic Process Research & Development

Year:

2008

File:

PDF, 26 KB

2008

19

Reduction of Ethyl Benzoylacetate and Selective Protection of 2-(3-Hydroxy-1-phenylpropyl)-4-methylphenol: A New and Facile Synthesis of Tolterodine

De Castro, Kathlia A., Ko, Jungnam, Park, Daejong, Park, Sungdae, Rhee, Hakjune

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 34 KB

english, 2008

20

A Review of U.S. Patents in the Field of Organic Process Development Published During August and September 2007

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 262 KB

english, 2008

21

An Integrated High-Throughput Screening Approach for Purification of Solid Organic Compounds by Trituration and Crystallization in Solvents

Tan, Helming, Reed, Maggie, Gahm, Kyung H., King, Tony, Seran, Mina Dilmeghani, Bostick, Tracy, Luu, Van, Semin, David, Cheetham, Janet, Larsen, Rob, Martinelli, Mike, Reider, Paul

Journal:

Organic Process Research & Development

Year:

2008

Language:

english

File:

PDF, 907 KB

english, 2008

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